2 documents found
Synchrotron X-ray nano-tomography datasets of unhydrated and 12, 16 and 20h hydrated tricalcium silicate particles
Reconstructed synchrotron X-ray nano-tomography (PXCT) datasets of unhydrated (0h) and hydrated (12h, 16h, 20 h) tricalcium silicate (C3S) embedded in epoxy resin. The C3S was sieved to a particle size <10 µm. For the hydration, 15 g of C3S was mixed with 45 g filtered, saturated Ca(OH)2-solution and…
A FIB-SEM Protocol for High-Resolution Imaging Combined with EDX Analysis of Cement-Based Materials with Minimized Damage
This is a recording of a talk held at the Microscopy Conference 2025 in Karlsruhe given on 4 September 2025. It shows how lift-out technique helps to avoid artefacts such as shadowing during the FIB nanotomography process and how post-processing is carried out for such a BSE+EDX data set. This dataset…